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Nov 17, 2021For the milling process, 40.12 g of the as-received Nb powder were loaded into two separate hardened steel containers of 125 ml volume with steel balls of 0.4 mm diameter, in a ball-to-powder
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Ball-milling reactions were performed in a MM400 mixer mill (Retsch , Haan, Germany), using a 5 mL stainless steel jar with four 5 mm diameter stainless steel balls and were milled vigorously at a frequency of 1800 rounds per minute (30 Hz) at room temperature. Aldoximes 1 were prepared according to the reported protocol .
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A promising approach in the selective separation and modification of cellulose from raw biomass under a mild alkali process was proposed. In our study, ball milling was applied to wheat straw prior to alkali treatment. With ball milling, ultrafine powder formed an amorphous microstructure and displayed a level of solubilization in aqueous NaOH higher than that of general ground
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Ball milling in organic synthesis: solutions and challenges † Achim Stolle,*a Tony Szuppa,a Silke E. S. Leonhardt a and Bernd Ondruschka a Author affiliations Abstract During the last decade numerous protocols have been published using the method of ball milling for synthesis all over the field of organic chemistry.
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